An improved digestion technique for determination of platinum group elements in geological samples | |
Liang Qi; Jianfeng Gao; Xiaowen Huang; Jing Hu; Mei-Fu Zhou; Hong Zhong | |
2011 | |
发表期刊 | Journal of Analytical Atomic Spectrometry |
卷号 | 26期号:9页码:1900-1904 |
摘要 | This paper reports a modified digestion method for the determination of platinumgroup elements (PGEs) in geological samples. Samples are first digested by HF in a custom made 120 ml PTFE beaker on a hot plate to remove silicates. The dried residue is then digested with HF + HNO3 at 190 °C for about 48 h after the beaker is sealed in a stainless steel pressure bomb. Although only HF + HNO3 are used for sample digestion at relatively low temperature, ultramafic rocks with refractory minerals can be effectively decomposed by this method. Analytical results for CCRMP (CANMET, Ottawa, Canada) certified reference materials WGB-1 (gabbro), UMT-1 (ultramafic ore tailings), WPR-1 (peridotite) and WMS-1(Massive Sulphide), agree well with the certified values. The proposed method significantly simplifies the sample digestion procedures for PGE analysis compared to those used previously. |
学科领域 | 矿床地球化学 |
收录类别 | SCI |
语种 | 英语 |
文献类型 | 期刊论文 |
条目标识符 | http://ir.gyig.ac.cn/handle/352002/7083 |
专题 | 矿床地球化学国家重点实验室_矿床地球化学国家重点实验室_期刊论文 矿床地球化学国家重点实验室 |
推荐引用方式 GB/T 7714 | Liang Qi,Jianfeng Gao,Xiaowen Huang,et al. An improved digestion technique for determination of platinum group elements in geological samples[J]. Journal of Analytical Atomic Spectrometry,2011,26(9):1900-1904. |
APA | Liang Qi,Jianfeng Gao,Xiaowen Huang,Jing Hu,Mei-Fu Zhou,&Hong Zhong.(2011).An improved digestion technique for determination of platinum group elements in geological samples.Journal of Analytical Atomic Spectrometry,26(9),1900-1904. |
MLA | Liang Qi,et al."An improved digestion technique for determination of platinum group elements in geological samples".Journal of Analytical Atomic Spectrometry 26.9(2011):1900-1904. |
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